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Process Research Methods

DOE and Parallel reaction 

Optimization of reaction conditions: reagent equivalent, temperature, concentration, reaction time, etc. 

It can significantly improve the efficiency of condition optimization and get the optimal condition quickly.

Destructive test (Stress test) 

It is essential to do destructive tests for laboratory-scale batches, including the stability of starting materials, intermediates and products. 

After the initial optimization of the process, it tests the applicable scope of the process.

The Spiking experiments 

Verify process performance, such as whether the spec setting is reasonable and whether impurities can be removed.